HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 21534851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 21534824 | HCID 21534824 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 21534851 | HCID 21534851 | 75.5% |
Reaction Steps
2-Methoxy-6-methylsulphonyl-10-(3-chloropropyl)phenothiazine (m.p. 122°-124°C.; 15.0 g.) is prepared by reacting 1-bromo-3-chloropropane (30.4 g.) with 2-methoxy-6-methylsulphonylphenothiazine (15.9 g.) in the presence of 85% pure ground potassium hydroxide (5.6 g.) dissolved in methyl ethyl ketone (75 cc.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961055 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-e665782cecba43519efbd5a8eed65c46 |
| Source note | uspto-grants-1976_06 |