HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21534860, compound → HCID 21534824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21534860 | HCID 21534860 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21534824 | HCID 21534824 | 35.7% |
Reaction Steps
2-Methoxy-6-methylsulphonylphenothiazine (m.p. 204°-206°C.; 16.05 g.) is prepared by reduction of 2-methoxy-6-methylsulphonyl-9-oxophenothiazine (47 g.) by means of zinc powder (28 g.) in dimethylformamide (175 cc.), acetic acid (73 cc.) and distilled water (73 cc.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961055 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-5465a5b2b11e4021abc8dc1dcadc7889 |
| Source note | uspto-grants-1976_06 |