HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → 2-Isopropoxy-6-dimethylsulphamoyl-10-(3-chloropropyl)phenothiazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | 2-Isopropoxy-6-dimethylsulphamoylphenothiazine | HCID 21534810 | — |
| Product | 2-Isopropoxy-6-dimethylsulphamoyl-10-(3-chloropropyl)phenothiazine | HCID 21534850 | 96.6% |
Reaction Steps
Crude 2-isopropoxy-6-dimethylsulphamoyl-10-(3-chloropropyl)phenothiazine (60.8 g.) is prepared by reacting 1-bromo-3-chloropropane (80.8 g.) with 2-isopropoxy-6-dimethylsulphamoylphenothiazine (m.p. 187°-189°C.; 52.0 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961055 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-e8495bff95054db6a66bc3af4b156904 |
| Source note | uspto-grants-1976_06 |