1-Bromo-3-chloropropane → HCID 21534859, compound

HRID 1657601Notes

Reaction equation

HRID 1657601 reaction equation
Br[CH2:2][CH2:3][CH2:4][Cl:5].[CH:6]([O:9][C:10]1[CH:23]=[CH:22][C:21]2[S:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][C:18]=3[S:24]([CH3:27])(=[O:26])=[O:25])[NH:13][C:12]=2[CH:11]=1)([CH3:8])[CH3:7]>>[CH:6]([O:9][C:10]1[CH:23]=[CH:22][C:21]2[S:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][C:18]=3[S:24]([CH3:27])(=[O:25])=[O:26])[N:13]([CH2:2][CH2:3][CH2:4][Cl:5])[C:12]=2[CH:11]=1)([CH3:8])[CH3:7]

Participants

3

Reactant 2

HCID 80061-Bromo-3-chloropropaneHCID 21534846HCID 21534846, compound

Product 1

HCID 21534859HCID 21534859, compoundYield 104.2%

Procedure

Crude 2-isopropoxy-6-methylsulphonyl-10-(3-chloropropyl)phenothiazine (128 g.) is prepared by reacting 1-bromo-3-chloropropane (100 g.) with 2-isopropoxy-6-methylsulphonylphenothiazine (m.p. 179°-180°C.; 100 g.).

Sources & evidence

ORD record
ord-9a082758263f423190a01523d769e617
Source dataset
uspto-grants-1976_06
Patent number
US03961055

Reaction notes

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