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HRID1657604

反应详情

EQUATION

反应方程式

HRID 1657604 的结构方程式

REACTANTS

反应物

3
结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：CCCCCCCI
HCID20274

Heptane, 1-iodo-

C7H15I

结构：CN(C)S(=O)(=O)c1cccc2c1Sc1ccc(O)cc1N2
HCID21534833

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCOc1ccc2c(c1)Nc1cccc(S(=O)(=O)N(C)C)c1S2
HCID21534838

未命名化合物

收率 149.8%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

2-Heptyloxy-6-dimethylsulphamoylphenothiazine (m.p. 160°-162°C.; 23.4 g.) is prepared by reacting 1-iodoheptane (8.4 g.) with 2-hydroxy-6-dimethylsulphamoylphenothiazine (76.8 g.) in the presence of powdered potassium hydroxide (41.4 g.) in methyl ethyl ketone (600 cc.).