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Potassium Hydroxide → 2-Heptyloxy-6-dimethylsulphamoylphenothiazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1-Iodoheptane | HCID 20274 | — |
| 反応物 | 2-Hydroxy-6-dimethylsulphamoylphenothiazine | HCID 21534833 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | 2-Heptyloxy-6-dimethylsulphamoylphenothiazine | HCID 21534838 | 149.8% |
反応手順
2-Heptyloxy-6-dimethylsulphamoylphenothiazine (m.p. 160°-162°C.; 23.4 g.) is prepared by reacting 1-iodoheptane (8.4 g.) with 2-hydroxy-6-dimethylsulphamoylphenothiazine (76.8 g.) in the presence of powdered potassium hydroxide (41.4 g.) in methyl ethyl ketone (600 cc.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03961055 |
| 出典データセット | uspto-grants-1976_06 |
| ORD ID | ord-e88a3f1c90944d6ca1c1af099f17619e |
| 出典メモ | uspto-grants-1976_06 |