HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarbonyl chloride → trans-1-(3-Phenylpropyl)-2,5-dimethyl-4-(2-furoyl)-piperazine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarbonyl chloride | HCID 68242 | — |
| Reactant | trans-1-(3-Phenylpropyl)-2,5-dimethylpiperazine | HCID 44361659 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | trans-1-(3-Phenylpropyl)-2,5-dimethyl-4-(2-furoyl)-piperazine hydrochloride | HCID 68131090 | — |
Reaction Steps
2-Furoyl chloride (13 g) was added dropwise to a solution of trans-1-(3-phenylpropyl)-2,5-dimethylpiperazine [b.p. 138 - 140 (4 mmHg), dipicrate, m.p. 258° - 261°C] (21 g) and benzene (200 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962249 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-13a227e3794f4171aa5ad848fac7edc1 |
| Source note | uspto-grants-1976_06 |