HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 21530920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 21530912 | HCID 21530912 | — |
| Reactant | HCID 21530917 | HCID 21530917 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21530920 | HCID 21530920 | — |
Reaction Steps
20 g of 3-chloro-4-chloromethylsulfonyloxy-phenylisocyanate (alternative name: chloromethanesulfonic acid 2-chloro-4-isocyanato-phenyl ester) were dissolved in 100 ml of acetone and 10 ml of a 45% strength dimethylamine solution were added, whilst cooling. After addition of water, N-(3-chloro-4-chloromethylsulfonyloxy-phenyl)-N,N'-dimethylurea precipitated: it was filtered off and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962306 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-df2920d8ca8c4e5e93b0ea973f604e57 |
| Source note | uspto-grants-1976_06 |