HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 2,6-Diethylacetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2,6-Diethylaniline | HCID 11369 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2,6-Diethylacetanilide | HCID 85534 | — |
Reaction Steps
A solution of 74.5 parts of 2,6-diethylaniline in 200 parts of dimethylformamide is treated with 56 parts of acetic anhydride at 10°C. The mixture is stirred at 40° for one hour, poured into ice and water and stirred. The solid 2,6-diethylacetanilide is filtered, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962307 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-00ce2b2afdf94aa8a020ec5a02a788b0 |
| Source note | uspto-grants-1976_06 |