反应详情

A solution of 74.5 parts of 2,6-diethylaniline in 200 parts of dimethylformamide is treated with 56 parts of acetic anhydride at 10°C. The mixture is stirred at 40° for one hour, poured into ice and water and stirred. The solid 2,6-diethylacetanilide is filtered, washed with water and dried.

1. stirringstirred
2. filtrationThe solid 2,6-diethylacetanilide is filtered
3. washwashed with water
4. customdried