HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-Nonen-1-yl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Nonanal | HCID 31289 | — |
| Reactant | Potassium Acetate | HCID 517044 | — |
| Product | 1-Nonen-1-yl acetate | HCID 53711837 | — |
Reaction Steps
A mixture of one mole of nonanal, 2.5 moles of acetic anhydride, and 15 g. of anhydrous potassium acetate is refluxed for one hour and cooled. Excess acid is removed by a 2X wash with water, followed by 5% sodium carbonate wash to give 1-nonen-1-yl acetate as a relatively pure oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962321 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-d28257bab0434f4d86b4b04a0ed7e4d2 |
| Source note | uspto-grants-1976_06 |