HRID1657937

反应详情

EQUATION

反应方程式

HRID 1657937 的结构方程式

PROCEDURE

实验过程

A mixture of one mole of nonanal, 2.5 moles of acetic anhydride, and 15 g. of anhydrous potassium acetate is refluxed for one hour and cooled. Excess acid is removed by a 2X wash with water, followed by 5% sodium carbonate wash to give 1-nonen-1-yl acetate as a relatively pure oil.

WORKUP

后处理

  1. temperaturecooled
  2. customExcess acid is removed by a 2X
  3. washwash with water
  4. washwash