HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 21529920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 21529911 | HCID 21529911 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21529920 | HCID 21529920 | — |
Reaction Steps
Isopropenyl azidoacetate (1.41 g, 0.01 mole) and anhydrous methanesulfonic acid (0.96 g, 0.01 mole) in 15 ml of methylene chloride is allowed to stand at room temperature for three hours. The solvent is removed in vacuo to give azidoacetyl methanesulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962224 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-20ad839bd24842a8851670aafa79381c |
| Source note | uspto-grants-1976_06 |