Methanesulfonic Acid → HCID 21529920, compound

HRID 1658007Notes

Reaction equation

HRID 1658007 reaction equation
[N:1]([CH2:4][C:5]([O:7]C(C)=C)=[O:6])=[N+:2]=[N-:3].[CH3:11][S:12](O)(=[O:14])=[O:13]>C(Cl)Cl>[CH3:11][S:12]([O:7][C:5](=[O:6])[CH2:4][N:1]=[N+:2]=[N-:3])(=[O:14])=[O:13]

Participants

4

Reactant 2

HCID 6395Methanesulfonic AcidHCID 21529911HCID 21529911, compound

Product 1

HCID 21529920HCID 21529920, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Isopropenyl azidoacetate (1.41 g, 0.01 mole) and anhydrous methanesulfonic acid (0.96 g, 0.01 mole) in 15 ml of methylene chloride is allowed to stand at room temperature for three hours. The solvent is removed in vacuo to give azidoacetyl methanesulfonate.

Workup

  1. customThe solvent is removed in vacuo

Sources & evidence

ORD record
ord-20ad839bd24842a8851670aafa79381c
Source dataset
uspto-grants-1976_06
Patent number
US03962224

Reaction notes

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