HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 21529934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | HCID 21529918 | HCID 21529918 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21529934 | HCID 21529934 | — |
Reaction Steps
A mixture of dibutyl N-benzyl-aminomethylphosphonate hydrochloride (122.4 g) and 10% palladium on powdered charcoal (5.0 g) in ethanol (1000 ml) is hydrogenated at 40 psi for 2 hours. The catalyst is removed by filtration and the filtrate is evaporated under reduced pressure to yield dibutyl aminomethylphosphonate hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962224 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-6b82dbcb97b2459087c7aa630d5e5ae7 |
| Source note | uspto-grants-1976_06 |