HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21529908, compound → HCID 12669615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21529908 | HCID 21529908 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12669615 | HCID 12669615 | — |
Reaction Steps
A mixture of diphenyl N-benzyl-aminomethylphosphonate hydrochloride (185.0 g), 10% palladium on carbon (7.0 g), and ethanol (1500 ml) is hydrogenated at 40 psi until hydrogen absorption ceases. The catalyst is removed by filtration through a pad of super cel and the filtrate is evaporated under reduced pressure to give diphenyl aminomethylphosphonate hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962224 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-08ab3f80ad7c4850b698052b95bdf365 |
| Source note | uspto-grants-1976_06 |