HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 54254034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-chloro-3-methoxypropan-2-one | HCID 20393050 | — |
| Reactant | HCID 86733537 | HCID 86733537 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54254034 | HCID 54254034 | — |
Reaction Steps
A mixture of p-nitrobenzyl α-thioformamidodiphenylphosphonoacetate (2.43 g), powdered potassium carbonate (0.73 ), 1-chloro-3-methoxy-2-propanone (0.63 g), and acetone (25 ml) is stirred in a capped flask at room temperature for 16 hours. The mixture is filtered and the filtrate is evaporated in vacuo to afford 3-methoxy-2-oxopropyl N-(p-nitrobenzyloxycarbonyl-diphenylphosphonomethyl)thioformimidate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962224 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-d7fa3866c2584946807ddbdbbf231bb2 |
| Source note | uspto-grants-1976_06 |