HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → 2-chloro-N-(2-chloro-4-sulfamoylphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | 4-Amino-3-chlorobenzenesulfonamide | HCID 1502014 | — |
| Product | 2-chloro-N-(2-chloro-4-sulfamoylphenyl)acetamide | HCID 21528830 | — |
Reaction Steps
2-Chloro-4-sulphamoylaniline (50 g) and α-chloroacetyl chloride (24 ml) were refluxed together for 45 min. and the product worked up as in Example 2(a) to yield 59.5 g, m.p. 162°-164°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-5724772342484e129e68f7fe4a05e641 |
| Source note | uspto-grants-1976_06 |