HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-Phenylamino-N-(2-bromo-4-sulphamoylphenyl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Chloro-N-(2-bromo-4-sulphamoylphenyl)-acetamide | HCID 21528844 | — |
| Product | 2-Phenylamino-N-(2-bromo-4-sulphamoylphenyl)-acetamide | HCID 21528869 | 80.6% |
Reaction Steps
2-Chloro-N-(2-bromo-4-sulphamoylphenyl)-acetamide (16.4g) and aniline (9.0 g) were heated together for 60 min. on a water bath at 90° the product was worked up as in Example 1(b) to yield 15,5 g beige crystals m.p.: 179°-181°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-7f522b9ec886475ab74dca5c6c79b908 |
| Source note | uspto-grants-1976_06 |