HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → S 332
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 2-Phenylamino-N-(2-methyl-4-sulphamoylphenyl)-acetamide | HCID 21528856 | — |
| Solvent | Water | HCID 962 | — |
| Product | S 332 | HCID 3041006 | — |
Reaction Steps
2-Phenylamino-N-(2-methyl-4-sulphamoylphenyl)-acetamide (16 g) was dissolved in ethano, (320 ml) and paraformaldehyde (1.9 g) in water (640 ml) added. The mixture was refluxed 11/2 hr, cooled and filtered. The residue was crystallised from DMF/water to yield 16 g, m.p. 206°-210°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-ca44e57fe5494e11997c588ad231df62 |
| Source note | uspto-grants-1976_06 |