HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Benzenesulfonamide, 3-chloro-4-(3-(4-methoxyphenyl)-5-oxo-1-imidazolidinyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 21528835 | HCID 21528835 | — |
| Solvent | Water | HCID 962 | — |
| Product | Benzenesulfonamide, 3-chloro-4-(3-(4-methoxyphenyl)-5-oxo-1-imidazolidinyl)- | HCID 3041011 | — |
Reaction Steps
The product of stage a) (15g) was dissolved in ethanol (200 ml) and treated with paraformaldehyde (2.5g) in water (400 ml). The mixture was refluxed for 3 hours, cooled in ice/water and filtered to yield the title product (5 g), m.p. 221°-223°
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-8f4ca76e6cc94683a5126b83062eb037 |
| Source note | uspto-grants-1976_06 |