HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → HCID 2990118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Acetanilide, 2-chloro-4'-nitro- | HCID 140220 | — |
| Solvent | Water ethylacetate | HCID 22728543 | — |
| Product | HCID 2990118 | HCID 2990118 | — |
Reaction Steps
2-Chloro-N-(4-nitrophenyl)-acetamide (11.5g) and cyclohexylamine (10.7g) were heated together 2 hours at 150° and then added to ethyl acetate/water. The product was extracted with ethyl acetate to yield 9.0g, m.p. 123°-125°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-07e88519ab6c47b38a4a6d0df4dc7220 |
| Source note | uspto-grants-1976_06 |