HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 21528832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | HCID 21528831 | HCID 21528831 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21528832 | HCID 21528832 | — |
Reaction Steps
2-Anilino-N-(4-sulphamoylphenyl)-acetamide (9.0 g) was heated with methyl chloroformate (30 ml) for 45 min. at 140°C. Work up from ethyl acetate/wate gave 7.0 g, m.p. 196° - 199°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-608f0adf10c74521be818670836e64ed |
| Source note | uspto-grants-1976_06 |