Methyl chloroformate → HCID 21528832, compound

HRID 1658230Notes

Reaction equation

HRID 1658230 reaction equation
[NH:1]([CH2:8][C:9]([NH:11][C:12]1[CH:17]=[CH:16][C:15]([S:18](=[O:21])(=[O:20])[NH2:19])=[CH:14][CH:13]=1)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[C:23]([O:25][CH3:26])=[O:24]>C(OCC)(=O)C>[CH3:26][O:25][C:23]([N:1]([C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[CH2:8][C:9]([NH:11][C:12]1[CH:17]=[CH:16][C:15]([S:18](=[O:21])(=[O:20])[NH2:19])=[CH:14][CH:13]=1)=[O:10])=[O:24]

Participants

4

Reactant 2

HCID 6586Methyl chloroformateHCID 21528831HCID 21528831, compound

Product 1

HCID 21528832HCID 21528832, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

2-Anilino-N-(4-sulphamoylphenyl)-acetamide (9.0 g) was heated with methyl chloroformate (30 ml) for 45 min. at 140°C. Work up from ethyl acetate/wate gave 7.0 g, m.p. 196° - 199°C.

Workup

  1. customgave 7.0 g, m.p. 196° - 199°C.

Sources & evidence

ORD record
ord-608f0adf10c74521be818670836e64ed
Source dataset
uspto-grants-1976_06
Patent number
US03963706

Reaction notes

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