HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfanilamide → HCID 21528866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfanilamide | HCID 5333 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Chloro-N-cyclohexylacetamide | HCID 222365 | — |
| Product | HCID 21528866 | HCID 21528866 | — |
Reaction Steps
2-Chloro-N-cyclohexylacetamide (8.7 g) and sulfanilamide (17.2g) were heated for 30 min. at 160°C. The mixture was then added to 2N NaOH and extracted with ethyl acetate to yield 8.2 g, product, m.p. 223° - 225°C
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-b3ccd198d17649e7bf02798452bfa3e8 |
| Source note | uspto-grants-1976_06 |