HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzenesulfonamide, 4-(3-cyclohexyl-2,4-dioxo-1-imidazolidinyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21528867 | HCID 21528867 | — |
| Solvent | Potassium Hydroxide | HCID 14797 | — |
| Product | Benzenesulfonamide, 4-(3-cyclohexyl-2,4-dioxo-1-imidazolidinyl)- | HCID 3050044 | 74% |
Reaction Steps
2-(N-Methoxycarbonyl-4-sulphamoylphenylamino)-N-cyclohexylacetamide (3.7 g) was dissolved in hot conc. KOH (15.0 ml). The solution was cooled and acidified with conc. HCl. The mixture was heated for 30 min. on a water bath and then filtered to yield 2.5 g product, m.p. 237° - 238°C (ethanol/water
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963706 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-9589c99114e34d4099d12e6e17974fe3 |
| Source note | uspto-grants-1976_06 |