HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylethanolamine → HCID 53636592, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | N-(1,4,5,6-Tetrahydropyrimidin-2-yl)nitramide | HCID 412214 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53636592 | HCID 53636592 | — |
Reaction Steps
A mixture of 7.2 parts of 1,4,5,6-tetrahydro-2-nitraminopyrimidine, 7.55 parts of α-(aminomethyl)benzyl alcohol and 12 parts of xylene is stirred and refluxed for 4 hours on a water-tap. The xylene is evaporated and the residue is dissolved in 20 parts of acetone. The product is crystallized at room temperature. It is filtered off and dried, yielding α-(1,4,5,6-tetrahydro-2-pyrimidinylaminomethyl)benzyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963718 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-626dce7b960c4c9e8428a5d63bdb6ae2 |
| Source note | uspto-grants-1976_06 |