HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Xylene → HCID 21510112, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | 3-Amino-1-phenylpropan-1-ol | HCID 121548 | — |
| Reactant | 2-Nitroamino-2-imidazoline | HCID 410042 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 21510112 | HCID 21510112 | — |
Reaction Steps
A mixture of 8 parts of α-(2-aminoethyl)benzylalcohol, 6.5 parts of 2-(nitramino)-2-imidazoline and 40 parts of xylene is stirred and refluxed for 3 hours with waterseparator. The reaction mixture is cooled and the separated oily product is dissolved in 4-methyl-2-pentanone. The solvent is evaporated in vacuo, yielding α-{2-[N-(2-imidazolin-2-yl)amino]ethyl} benzylalcohol as a residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963718 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-8a4fd903ff8a44df81d1b4350f2168dd |
| Source note | uspto-grants-1976_06 |