HRID1658277

反应详情

EQUATION

反应方程式

HRID 1658277 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 3.0 g. of 4-nitrobenzofuran, 0.5 g of 5% Rhodium on carbon and 25 ml. of ethanol is hydrogenated in a Parr apparatus at a hydrogen pressure of 50 p.s.i. and temperature of 35°C. until the uptake of hydrogen ceases. The catalyst is removed by filtration and the filtrate evaporated in vacuo to obtain an oil of 2,3-dihydro-4-benzofuranamine.

WORKUP

后处理

  1. additionA mixture of 3.0 g
  2. customtemperature of 35°C.
  3. customThe catalyst is removed by filtration
  4. customthe filtrate evaporated in vacuo