HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 2,2,6,6-Tetramethyl-4-piperidone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Ammonium Bromide | HCID 25514 | — |
| Reactant | Acetonin | HCID 68396 | — |
| Product | 2,2,6,6-Tetramethyl-4-piperidone | HCID 13220 | 239% |
Reaction Steps
5 g. of Acetonine and 12.4 g. of ammonium bromide were added to 30 g. of acetone and the mixture was maintained at room temperature for 38 hours to effect the reaction. After completion of the reaction, the reaction mixture was purified in the same manner as in Example 1 to obtain triacetonamine in a yield of 239%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963730 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-021414862aa7489e8e7d61e2e879d530 |
| Source note | uspto-grants-1976_06 |