HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21529154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21529152 | HCID 21529152 | — |
| Product | HCID 21529154 | HCID 21529154 | — |
Reaction Steps
A suspension of 5 g. of 3-(p-methoxybenzylthio)-picolinamide in 50 ml. of 20% aqueous sodium hydroxide is refluxed for about 24 hours, then cooled and acidified with dilute hydrochloric acid. Filtering, washing the precipitate with water, drying and recrystallizing from methanol gives 3-(p-methoxybenzylthio)picolinic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963733 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-d78ac1db06aa43feba56acf0aac5c7b4 |
| Source note | uspto-grants-1976_06 |