HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 3504015, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Ethyl 8-ethoxy-2H-[1,3]dioxolo[4,5-g]quinoline-7-carboxylate | HCID 12367717 | — |
| Product | HCID 3504015 | HCID 3504015 | — |
Reaction Steps
A melt of 5 g of ethyl 4-ethoxy-6,7-methylenedioxyquinoline-3-carboxylate was heated at 220°C for 7 hours and then cooled. The product was thinned with toluene, filtered and recrystallized from chloroform petroleum ether to provide 3.7 g of ethyl 1-ethyl-6,7-methylenedioxy-4-quinolone-3-carboxylate as needles, m.p. 177°-178°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963736 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-e2b380fc8adb4a44b68f483c513f17ed |
| Source note | uspto-grants-1976_06 |