Methyl iodide → AGN-PC-00J94Q

HRID 1658425Notes

Reaction equation

HRID 1658425 reaction equation
[CH3:1][I:2].[NH2:3][N:4]1[CH2:9][CH2:8][O:7][CH2:6][CH2:5]1>CCOCC>[I-:2].[NH2:3][N+:4]1([CH3:1])[CH2:9][CH2:8][O:7][CH2:6][CH2:5]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 20315N-Aminomorpholine

Product 1

HCID 11984517AGN-PC-00J94QYield 96%

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A 12.78-g (0.09 mole) sample of methyl iodide was added dropwise to a solution of 8.6 g (0.084 mole) of N-aminomorpholine in 50 ml ether. The precipitate that formed was collected on a filter, washed with ether and dried in air to give 19.73 g (96% yield) of N-amino-N-methylmorpholinium iodide as colorless crystals, mp 150°-155°(d).

Workup

  1. customThe precipitate that formed
  2. customwas collected on a filter
  3. washwashed with ether
  4. customdried in air

Sources & evidence

ORD record
ord-31e64c1c34964b1aba2890272a2b740f
Source dataset
uspto-grants-1976_06
Patent number
US03963776

Reaction notes

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