HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → AGN-PC-00J94Q
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | N-Aminomorpholine | HCID 20315 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | AGN-PC-00J94Q | HCID 11984517 | 96% |
Reaction Steps
A 12.78-g (0.09 mole) sample of methyl iodide was added dropwise to a solution of 8.6 g (0.084 mole) of N-aminomorpholine in 50 ml ether. The precipitate that formed was collected on a filter, washed with ether and dried in air to give 19.73 g (96% yield) of N-amino-N-methylmorpholinium iodide as colorless crystals, mp 150°-155°(d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03963776 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-31e64c1c34964b1aba2890272a2b740f |
| Source note | uspto-grants-1976_06 |