HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 21527620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | HCID 13066242 | HCID 13066242 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 21527620 | HCID 21527620 | — |
Reaction Steps
3 g of 4-(2,3-epoxypropoxy)oxindole, 30 cc of allylamine and 70 cc of dioxane are heated to the boil for 16 hours. The mixture is evaporated to dryness at reduced pressure and the crude title compound is recrystallized from ethanol/ethyl acetate. M.P. 124°-127° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965095 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-80e0a3b6fc68471a92f68b6237f5d798 |
| Source note | uspto-grants-1976_06 |