HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium amide → HCID 21881801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium amide | HCID 24533 | — |
| Reactant | 3,4-Diethylpyridine | HCID 69151 | — |
| Product | HCID 21881801 | HCID 21881801 | — |
Reaction Steps
2-Amino-3,4-diethylpyridine is prepared by reacting 40.5 g. 3,4-diethylpyridine with 11.7 g sodium amide at a temperature of 250° in the presence of paraffin oil. The so-formed 2-amino-3,4-diethylpyridine is purified by distillation and is substituted for the 2-amino-3,4-dimethylpyridine in Example 7 to obtain the named compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965100 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-04184831477e4b13bb8751fbe033f4c8 |
| Source note | uspto-grants-1976_06 |