Sodium amide → HCID 21881801, compound

HRID 1658507Notes

Reaction equation

HRID 1658507 reaction equation
[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH2:9][CH3:10])[CH3:2].[NH2-:11].[Na+]>>[NH2:11][C:4]1[C:3]([CH2:1][CH3:2])=[C:8]([CH2:9][CH3:10])[CH:7]=[CH:6][N:5]=1

Participants

3

Reactant 2

HCID 24533Sodium amideHCID 691513,4-Diethylpyridine

Product 1

HCID 21881801HCID 21881801, compound

Procedure

2-Amino-3,4-diethylpyridine is prepared by reacting 40.5 g. 3,4-diethylpyridine with 11.7 g sodium amide at a temperature of 250° in the presence of paraffin oil. The so-formed 2-amino-3,4-diethylpyridine is purified by distillation and is substituted for the 2-amino-3,4-dimethylpyridine in Example 7 to obtain the named compound.

Workup

  1. customat a temperature of 250°
  2. distillationThe so-formed 2-amino-3,4-diethylpyridine is purified by distillation
  3. customto obtain the named compound

Sources & evidence

ORD record
ord-04184831477e4b13bb8751fbe033f4c8
Source dataset
uspto-grants-1976_06
Patent number
US03965100

Reaction notes

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