HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → 2-Phenylethylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 5-Chloro-2-methoxybenzoyl chloride | HCID 12384176 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-Phenylethylamine hydrochloride | HCID 9075 | — |
Reaction Steps
5-Chloro-2-methoxybenzoyl chloride (15g.), dissolved in benzene, was added slowly to a solution of phenethylamine (18 g.) in benzene. Phenethylamine hydrochloride formed was filtered off, and the benzene removed from the filtrate. The residual oil was distilled to give an oil (19.4 g., 90%) b.p. 205° at 0.2 mm., which crystallized on standing m.p. 60°-63°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965173 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-d9dba61bbd8e46a5aa91ddc19d9e826a |
| Source note | uspto-grants-1976_06 |