HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → 4-Methylphenyl phosphorodichloridate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Product | 4-Methylphenyl phosphorodichloridate | HCID 248905 | — |
Reaction Steps
To a mixture of 225 g. phosphoryl chloride and methylamine there is added 109 g. cresol over a period of 2 hours at a temperature of 105°C. The temperature is held at 105°-110°C. for two hours to afford cresyl phosphorodichloridate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03965220 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-5f7e99a2500f40eb89c7d01d3d293f9a |
| Source note | uspto-grants-1976_06 |