HRID1658698

反应详情

EQUATION

反应方程式

HRID 1658698 的结构方程式

PROCEDURE

实验过程

N-Methoxyquinolinium p-toluenesulfonate was prepared by mixing quinoline-N-oxide and an equimolar amount of methyl p-toluenesulfonate and heating the mixture at 95°C for 5 hours. The crude product was recrystallized from a mixture of methanol and ethyl acetate. By this procedure N-methoxyquinolinium p-toluenesulfonate was obtained. The salt had the following features in the NMR:

WORKUP

后处理

  1. customN-Methoxyquinolinium p-toluenesulfonate was prepared
  2. customThe crude product was recrystallized from a mixture of methanol and ethyl acetate