HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfide → HCID 11745097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfide | HCID 1068 | — |
| Reactant | Methyl Methanesulfonate | HCID 4156 | — |
| Product | HCID 11745097 | HCID 11745097 | — |
Reaction Steps
A mixture of 1.24 g of dimethylsulfide and 2.20 g of methyl methanesulfonate was allowed to stand for three days at room temperature. The crystals which deposited were collected by filtration, washed with diethyl ether and dried. By this procedure crystals of S,S,S-trimethylsulfonium methanesulfonate were obtained. When this product was recrystallized, it had a melting point of 193.0° to 195.0°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966720 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-ddda0e3cdc3442c79f6f56766ae37a15 |
| Source note | uspto-grants-1976_06 |