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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1658718Generated: October 30, 2026

Methylamine → HCID 70636802, compound

https://huagongshe.com/reaction/1658718

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 70637887HCID 70637887—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 70636802HCID 70636802—

Reaction Steps

1 g of 2-keto-1,2,3,4,10,14b-hexahydro-pyridino[1,2-a]-dibenzo[c,f]-azepine is dissolved in 100 ml of ethanol, after which 10 ml of methylamine and 200 mg of palladium (10%) on charcoal are added. Then hydrogen is passed through this mixture until no hydrogen is absorbed any longer.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03966723
Source datasetuspto-grants-1976_06
ORD IDord-640268115d3a4cf9b77a168aedc6fda3
Source noteuspto-grants-1976_06