HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl formate → HCID 70637047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl formate | HCID 7865 | — |
| Reactant | HCID 86733599 | HCID 86733599 | — |
| Solvent | Aceton-methanol | HCID 21894497 | — |
| Product | HCID 70637047 | HCID 70637047 | — |
Reaction Steps
The above-mentioned product is treated with methylformate in the same way once again (melting point N-formyl-N-methylamino-methyl compound: 117°-119°C) and reduced after that. Obtained in this manner: 3.4 g. Melting point (ax.): 2-dimethylaminomethyl-1,2,3,4,10,14b-hexahydro-pyridino[1,2-a]-dibenzo[c,f]-azepine fumarate: 174°-176°C. Rf in methanol:acetone (9:1) = 0.40 on SiO2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966723 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-6c324d8192324766af1ecab2ac0d3603 |
| Source note | uspto-grants-1976_06 |