HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21525460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21525466 | HCID 21525466 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21525460 | HCID 21525460 | — |
Reaction Steps
0.2 g. of 5-(2-acetoxyethoxy)-2-(5-nitro-1-methyl-2-imidazolyl)-pyrimidine is refluxed in 5 ml. of ethanol with 2.5 ml. of concentrated hydrochloric acid. After concentration under vacuum, the residue is recrystallized from ethyl acetate; m.p. 158°-160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966732 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-39e6f0d7b7ed4e53b8a09ab28a893419 |
| Source note | uspto-grants-1976_06 |