Hydrochloric Acid → HCID 21525460, compound

HRID 1658728Notes

Reaction equation

HRID 1658728 reaction equation
C([O:4][CH2:5][CH2:6][O:7][C:8]1[CH:9]=[N:10][C:11]([C:14]2[N:15]([CH3:22])[C:16]([N+:19]([O-:21])=[O:20])=[CH:17][N:18]=2)=[N:12][CH:13]=1)(=O)C.[ClH:23]>C(O)C>[ClH:23].[OH:4][CH2:5][CH2:6][O:7][C:8]1[CH:13]=[N:12][C:11]([C:14]2[N:15]([CH3:22])[C:16]([N+:19]([O-:21])=[O:20])=[CH:17][N:18]=2)=[N:10][CH:9]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21525466HCID 21525466, compound

Product 1

HCID 21525460HCID 21525460, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

0.2 g. of 5-(2-acetoxyethoxy)-2-(5-nitro-1-methyl-2-imidazolyl)-pyrimidine is refluxed in 5 ml. of ethanol with 2.5 ml. of concentrated hydrochloric acid. After concentration under vacuum, the residue is recrystallized from ethyl acetate; m.p. 158°-160° C.

Workup

  1. concentrationAfter concentration under vacuum
  2. customthe residue is recrystallized from ethyl acetate

Sources & evidence

ORD record
ord-39e6f0d7b7ed4e53b8a09ab28a893419
Source dataset
uspto-grants-1976_06
Patent number
US03966732

Reaction notes

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