HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4-Fluorobenzoyl)propyl chloride → HCID 68130838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4-Fluorobenzoyl)propyl chloride | HCID 19750 | — |
| Reactant | HCID 409099 | HCID 409099 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68130838 | HCID 68130838 | — |
Reaction Steps
A 1.0 g. portion of γ-chloro-p-fluorobutyrophenone and 0.9 g. of 4-(4-methyl-2-thiazolyl)pyridine are heated in an oil bath at 95°-100°C. overnight. Ether is added and the mixture is filtered. The solid is recrystallized from acetonitrile. This solid is recrystallized from a mixture of alcohol and ether, m.p. 226°-228°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966748 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-5559e48beb294fa8bfa793548511873d |
| Source note | uspto-grants-1976_06 |