HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 21525721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 12268147 | HCID 12268147 | — |
| Reactant | ethanol water DMF | HCID 86633292 | — |
| Product | HCID 21525721 | HCID 21525721 | — |
Reaction Steps
Following a procedure similar to that described in Example 1 and using 5-amino-10,11-dihydro-5H-dibenz[b,f]-azepine hydrochloride (5g.) and B-phthalimidopropaldehyde (4.1g.) in glacial acetic acid (75 ml.) there was obtained N-[(6,7-dihydroindolo[1,7-ab][1]benzazepine-2-yl)methyl] phthalimide (5.0g.), m.p. 190°-191°C. (dimethylformamide-ethyl alcohol-water/7.5:1:3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966762 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-2ee8709ccb6c454cabda22890680cec0 |
| Source note | uspto-grants-1976_06 |