Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Product | Methyl sorbate | HCID 5323650 | — |
Reaction Steps
A quantity of 1.1 grams palladium acetate, 0.61 cc-47° by weight hydrogen bromide, 5.25 grams triphenyl phosphine, 45 cc allyl alcohol, and 60 cc methyl acrylate is introduced into a reaction chamber and heated to 120°C for a period of 15 hours. Methyl sorbate is produced to the extent of 15% by weight of the final reaction solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03966798 |
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| Source dataset | uspto-grants-1976_06 |
|---|
| ORD ID | ord-8403e7f1fcce47118fc1e18c87fdea11 |
|---|
| Source note | uspto-grants-1976_06 |
|---|
