HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1658902Generated: October 27, 2026
Hydrogen Bromide → 2-Propenoic acid, 3-phenyl-, methyl ester
https://huagongshe.com/reaction/1658902
Participants
| Role | Name | HCID | Charge |
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| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Catalyst | palladium(II) acetate | HCID 167845 | — |
| Product | 2-Propenoic acid, 3-phenyl-, methyl ester | HCID 7644 | — |
| Product | Methyl sorbate | HCID 5323650 | — |
| Product | Allyl sorbate | HCID 6435833 | — |
Reaction Steps
Quantities of 5 millimoles palladium acetate, 20 millimoles triphenyl phosphine, 5 millimoles of hydrogen bromide, 600 millimoles allyl alcohol, and 600 millimoles methyl acrylate are introduced into a reaction chamber and heated to 135°C for 20 hours. The final reaction solution produced 15% by weight methyl sorbate, allyl sorbate, and traces of methyl cinnamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US03966798 |
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| Source dataset | uspto-grants-1976_06 |
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| ORD ID | ord-b7841dbc5b3f4c0d944dbee568bac915 |
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| Source note | uspto-grants-1976_06 |
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