HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53795161, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis- | HCID 11076276 | — |
| Reactant | HCID 21316300 | HCID 21316300 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53795161 | HCID 53795161 | — |
Reaction Steps
In a manner similar to that described in Example 5, treat the cyclic diamine obtained in Example 45 and triethylamine in anhydrous benzene with 1,2-di-(chlorocarbonylmethoxy)-benzene (compound of Example 61) utilizing high dilution technique. Isolate and purify the resultant product in a manner similar to that described in Example 5 to obtain 2,13-dioxo-4,11,17,22-tetraoxa-1,14-diaza-tricyclo[12,5,5,05,10 ]tetracosa-5,7,9-triene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966766 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-3c61811b6ab046b18a2238f9d8635461 |
| Source note | uspto-grants-1976_06 |